HR: 14:25h
AN: A53E-04 [Abstracts]
TI: Speciated Organic Composition of Atmospheric Aerosols: A New, In-Situ Instrument
AU: * Williams, B J
EM: brentw@nature.berkeley.edu
AF: University of California - Berkeley, ESPM Ecosystem Sci. Division
151 Hilgard Hall, Berkeley, CA 94720-3110
United States
AU: Goldstein, A H
EM: ahg@nature.berkeley.edu
AF: University of California - Berkeley, ESPM Ecosystem Sci. Division
151 Hilgard Hall, Berkeley, CA 94720-3110
United States
AU: Hering, S V
EM: susanne@aerosol.us
AF: Aerosol Dynamics Inc., 2329 4th St, Berkeley, CA 94710
United States
AU: Kreisberg, N M
EM: nathan@aerosol.us
AF: Aerosol Dynamics Inc., 2329 4th St, Berkeley, CA 94710
United States
AB:
Identification and quantification of the organic composition of ambient atmospheric aerosols is key to tracking sources of
aerosols which impact human health, atmospheric visibility, and global climate. Organic matter is a major constituent of
airborne particles, comprising 20-50% of the mass of airborne particles below 2.5 æm in diameter. The composition is
complex, with hundreds of compounds identified through chromatographic mass spectrometry techniques. While the identified
compounds only comprise a fraction of the total organic mass, those that are quantified serve as valuable tracers for
sources. For example, hopanes, which are remnants of the biological material from which petroleum originated, serve as a
unique tracer for fossil fuel combustion. Levoglucosan is a product of the breakdown of cellulose, and is a unique tracer
for wood combustion. A substantial limitation in the use of organic marker compounds for source identification is the
difficulty, and cost of the analyses. Needed are time-resolved, cost-effective measurements of specific organic marker
compounds.
Reported here are initial results from a new, in-situ instrument, the Thermal desorption Aerosol GC-MS/FID (TAG). This is an
automated instrument for the time-resolved identification and quantitation of selected organic marker compounds in airborne
particles over the size range from 0.1 to 2.5 æm. Atmospheric aerosol samples are collected into a thermal desorption cell
by means of humidification and impaction. The sample is transferred onto a GC column by thermal desorption, with subsequent
GC-MS/FID analysis. The collection and analysis steps are automated, yielding around the clock speciation. A droplet
injector is being developed to provide internal standards for each sample. An advantage of our approach is that it builds on
the extensive body of knowledge on the quantification of organic material, and on the identification of the origins of
organic aerosols available from past research using filter-based GC/MS analyses. Initial results of ambient aerosol
measurements made at Chebogue Point, Nova Scotia, Canada from July-August 2004 during the International Consortium for
Atmospheric Research on Transport and Transformation (ICARTT 2004) study will be presented.
DE: 0305 Aerosols and particles (0345, 4801)
DE: 0315 Biosphere/atmosphere interactions
DE: 0322 Constituent sources and sinks
DE: 0345 Pollution--urban and regional (0305)
DE: 0368 Troposphere--constituent transport and chemistry
SC: Atmospheric Sciences [A]
MN: 2004 AGU Fall Meeting